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, Experimental Part 1. Infra Red Spectroscopy Infra-red spectra were acquired using an ATR-FTIR spectrometer

X. , Powder Diffraction (XRPD)

, XRPD analyzes were performed using a D8-Discover diffractometer

, Temperature Resolved X-Ray Powder Diffraction (TR-XRPD)

. Tr-x-, Ray diffraction analyses were performed using a D5005 diffractometer

, X-ray beam is generated by a sealed Cu Source (40 kV, 40 mA), and a K? filter

, Thermogravimetry Differential Scanning Calorimetry

, TG-DSC analyses are carried out with a STA 409 PC instrument (Netzsch). The DSC and TGA signal are plotted against temperature

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