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, époxy a été déterminée par la méthode de la goutte posée à l'aide d'un goniomètre GBX. A partir des mesures des angles de contact avec l'eau et le diiodométhane en tant que liquides sondes sur les échantillons, les composantes polaire et dispersive de l'énergie de surface ont été déterminées en utilisant la théorie
, Le spectre d'absorption infrarouge à transformée de Fourier a été obtenu à l'aide d'un
, Analyse mécanique dynamique (AMD)
, L'analyse mécanique dynamique est effectuée sur des échantillons rectangulaires avec une
, Caractérisations diélectriques La caractérisation diélectrique du réseau époxy a été effectuée sur un spectromètre diélectrique AMETEK Solartron analytical (Modulab XM MTS), équipé d'une sonde de température complexe *. La conductivité AC (? AC ) peut être extrapolée à partir d'une partie réelle de la conductivité ?'(?) = ? 0 ''(?) pour ? ?
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, Dans ce cas présent, le monomère LI 45b semble particulièrement réactif comparé à la DGEBA. Concernant la largeur du pic exothermique comprise entre 50 et 195 °C dans le cas du monomère LI, elle est similaire à celle des systèmes époxy-amine classiques
, En effet, l'exothermie du système DGEBA-D230 'état initial, l'énergie d'activation d'un système DGEBA/D230 diminue pour un degré de polymérisation (?)
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, ces résultats prometteurs permettent d'ouvrir de nouvelles perspectives dans la préparation de revêtements hydrophobes voire anti-corrosion par le remplacement des prépolymères époxydes communs
, Conductivité ionique du réseau époxy Depuis plusieurs années, beaucoup de travaux sont dédiés au développement d'électrolytes polymères gélifiés ou solides pour des applications énergétiques. 203 Ainsi, de nombreux polymères sont utilisés en tant qu'« hôte » tels que l'oxyde de polyéthylène (PEO), le poly(fluorure de vinylidène) (PVDF) et de nombreux PILs. 6b,204 Néanmoins, la majorité des électrolytes basés sur des
,
, S.m -1 à 30 °C. 207 Récemment, Porcarelli et al. ont synthétisé de nouveaux LI comme des monomères méthacryliques copolymérisés avec le poly(éthylène glycol) méthyl éther méthacrylate et ont obtenu des polymères électrolytes solides avec, °C. 206 D'autres auteurs ont mis au point un poly(diallylammonium) chlorure contenant 10 % en masse de LI et montrant une conductivité ionique de 9, pp.10-17
, Dans le but de déterminer le potentiel du nouveau réseau époxy 45b/D230 en tant qu'électrolyte polymère, la conductivité ionique de ce réseau a ainsi été mesurée à différentes températures en fonction de la fréquence, vol.47
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, (m, 6H, H-4, H-4', H-5), 2.11-2.27 (m, 2H, H-2, H-2'), 1.87-1.98 (m, 2H, H-2, H-2'), 1.40-1.50 (m, 2H, H-6), 1.25-1.36 (m, 2H, 500 MHz) . -8.08 (m, 2H, N-CH), 7.83-7.86 (m, 2H, N-CH), vol.123, 1051.
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