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, To this end, collected gas samples in nalophan bags were directly pumped into a 400 µL loop injection valve at a flow rate of 100 mL min -1 . The looped gases were then injected into a capillary column (1.2 m x 1.6 mm x 180 µm) with air as carrier gas at a flow of 4 mL min -1 . A column pressure of 230 hPa and a column temperature of 40 °C were held constant throughout the analysis. After separation, VSC were transferred toward an electrochemical cell composed of two platinum electrodes submerged in chromic oxide solution, GC coupled to an electrochemical detector (airMEDOR, vol.6326, 1981.
, Quantification of VSC was achieved by external calibration (R 2 = 0.94-0.99) with high purity compounds (> 98.5%; Sigma-Aldrich and Across Organics) and standard gas cylinders, 201±7 ppm and 207±10 ppm standards of H2S and CH3SH
, The trapped VOC were then desorbed in the thermal desorption unit at 200°C for 5 min and transferred toward the CG/MS. Once injected, VOC were separated in a capillary column CP-WAX 58 (25m x 0.15 mm x 0.25µm, Varian, USA) with helium as a carrier gas (1 mL min -1 ) and a column pressure of 310 kPa. The GC oven temperature was first held at 40 °C for 5 min, then increased to 180 °C at 10 °C min -1 , and finally maintained at 180 °C for 5 min. VOC were identified by comparing obtained mass spectra (20 to 300 amu) with reference entries from a spectral mass library (NIST 2012, National Institute of Standards and Technology, USA). Moreover, retention times provided a useful criterion for identification if chemical standards were available. The compounds peaks and the identified diagnostic ions (m/z) were acquired and integrated into a full scan and single ion monitoring (SIM) mode. An example of a chromatogram obtained during GC/MS analysis of gas emission is provided in Fig 1S (Supplementary material). An external calibration process (R 2 = 0.92-0.99) was applied to quantify VOC with standards (Purity > 98%, suppliers: Fluka, The gas samples collected in nalophan bags were first adsorbed onto sorbent tubes (Carbotraps 349, Perkin Elmer, USA) at a flow rate of 52 mL min -1 with a calibrated vacuum pump (Gilair3, USA), vol.550
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