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, Conclusions et Perspectives Les sondes à NTC présentent de nombreux avantages dont l'amélioration de la durée de vie de la sonde et l'aptitude à imager à haute résolution des échantillons dans l'air et l'eau. Leur déploiement industriel à grande échelle est toutefois limité par les contraintes de fabrication (contrôle de l'orientation et de la taille du NTC, faible rendement, coût de production élevé). C'est pourquoi l'analyse des méthodes de synthèse et l
, Annexe 2 : Paramètres des synthèses de NTC mono-paroi
, Chaque ligne correspond aux paramètres d'une synthèse réalisée au cours de cette thèse
, Du fait du grand nombre de paramètres, la lecture de ce tableau peut être difficile sur papier. La visualisation est plus facile en version électronique de la thèse
, Annexe 3 : Technique d'analyse dispersive en énergie (EDX)
, La technique d'analyse dispersive en énergie (EDX ou EDS) est généralement combinée à la microscopie électronique. Un faisceau électron de haute énergie est envoyé sur l'échantillon
, Une ionisation entraîne la création d'une paire d'électron-trou. Un champ électrique permet de collecter les électrons et ainsi de déterminer le nombre d'ionisations. Grâce à l'étalonnage du détecteur, ce nombre est ensuite converti en énergie pour le photon incident. L'intensité des rayons X est proportionnelle à la fraction de l'élément présent dans l'échantillon. La résolution de l'analyse, Suite aux ionisations et excitations de l'échantillon induites par le faisceau, les atomes impactés détecteurs utilisés sont souvent des semi-conducteurs
, La précision de la technique EDX est de quelques pourcentages de la composition totale
, Un élément peut émettre plusieurs pics caractéristiques (tels que K?, K? ...) correspondant