Le récipient est placé dans une clocheà vide pendant une vingtaine de minutes pour retirer les bulles d'air introduites pendant le mélange. Le PDMS encore liquide est spin-coaté sur un waferà une vitesse de 2000 rpm pendant 30 secondes. Une fois cetteétape réalisée, préparé de la même manière que pour les puces microfluidiques. On mélange du PDMS et son réticulant dans les proportions, vol.10, p.65 ,
Après un délai minimal d'une heure, le wafer est prêtàêtre utilisé ,
, Ce protocole permet de déposer une couche de PDMS d'environ 15 µm sur les wafers
, Cette valeur aété déterminéeà l'aide d'un profilomètre mécanique (Dektak)
, Du scotch a aussiété utilisé pour retirer les poussières ou les dépôts formés par le séchage des gouttes. Son utilisation aété limitée aux expériences du chapitre 2. Les expériences de mesures de contraintes dans les chapitres 3 et 4étaient en effet affectées par l, Les poussières adhèrent fortement au PDMS qui se salit rapidement
, En s'évaporant, le solvant laisse un film fin et transparent. Ce film a de bonnes propriétés hydrophobes. La solution est peu différentes, notammentà hautes concentrations, car dans ce régime
, Il est intéressant de noter que même pour des fractions vos ? 0.3) : c'est l'exclusion de Donnan. Les nanoparticules sont si chargées qu'elles excluent la majorité des contre-ions ajoutés dans le réservoir. C'est une différence majeure avec les cas expérimentaux traités dans le manuscrit (goutte vs. micropervaporateur), voir discussions dans la conclusion des chapitres 1 et 2, La figure C.2 (c) montre quantà elle la concentration moyenne en sels dans la dispersion (voiréquation C.4), pp.53-84
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