, Chapitre I : Matériels et Méthodes, vol.75

, une enceinte étanche permettant de maîtriser l'atmosphère de l'échantillon

, un four permettant de gérer la température

, un module de pesée (microbalance)

, un thermocouple pour mesurer la température

, Ainsi qu'un ordinateur permettant de piloter l'ensemble, pour faire l'acquisition des données et le traitement des résultats

, Annexe 6 : Chromatographie liquide à haute performance (CLHP)

, Le résidu sec résultant est solubilisé dans un mélange constitué de 1 mL de THF (tétrahydrofurane) et 1 mL d'acétonitrile (ACN), puis filtré sur un filtre téflon millipore (0,22 µm) et injecté. Dans les ENC mis en contact avec le toluène, ces derniers sont évaporés et les résidus secs respectifs, en CLHP est faite après extraction par dissolution-précipitation du COC

, Nous avons utilisé un système Ultramate 3000 (Dionex) composé d'un injecteur automatique, d'une pompe et d'un détecteur UV-Visible à longueur d'onde variables

, µL de solution à analyser sont injectés sur une colonne de type LiChrocart® 250-4 RP-18e

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. Low and R. T. Limit,

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