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, Afin de réaliser les mesures d'ATG-DSC, le protocole suivant a été employé
, Montée en température jusqu'à 250°C avec une vitesse de chauffage de 10°C/min
, Au début du chauffage, le débit d'azote est ramené à 20 ml/min et est maintenu ainsi jusqu'à la fin de l'expérimentation