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. Ii, Ordered mesoporous silica: SBA-15 and SBA-16 type materials

B. , Preparation of SBA-15 type materials

C. , Functionalization of amorphous and ordered mesoporous silica with TEMPO moieties, vol.84

. Iv, Hybrid ordered mesoporous silica containing TEMPO radicals

A. , Preparation of precursors and multi-step synthesis leading to ordered mesoporous silica coated with TEMPO moieties

B. , Characterization of the hybrid ordered silica materials

S. ). , Evaluation and quantification of the species on the surface: EPR analysis and DRIFT spectroscopy

. , 106 1. Preparation of ordered mesoporous silica for d-DNP experiments

. , 107 4. 1 H polarization transfer to carbon nuclei using cross-polarization in HYPSO 3 as polarizing matrix, 110 5. Investigation of the build-up times of HYPSO materials

V. .. Conclusions,

B. , Diffuse Reflectance Infrared Fourrier Transform Spectroscopy (DRIFTS)

. , Continuous Wave Electron Paramagnetic Resonance (CW EPR) parameters and

E. Nuclear, Magnetic Resonance (NMR)

S. .. ,

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