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, ANNEXE, vol.1

A. Chimique and «. Beraha,

D. De, . De, . Bandes, . Dans-l-'epaisseur, and . De, Afin que l'attaque soit de bonne qualité, il est fortement conseillé qu'un polissage miroir (1 µm) de la surface à attaquer soit réalisé au maximum quelques heures avant. La composition de la solution d'attaque est la suivante : -0,3 g de bisulfite de potassium HKSO? -20 mL d'acide chlorydrique HCl -100 mL d'eau déionisée H 2 O La procédure d'attaque consiste à placer la solution dans un bécher et, avec une pince, venir tremper la surface à révéler quelques secondes. La durée d'attaque est très variable, même pour un même type d'échantillon. Il est important d'observer attentivement et la surface de l'échantillon dès lors que celui-ci est immergé. La fin de l'attaque est marquée par un changement de couleur de la surface, qui devient très légèrement jaunâtre. Il est conseillé de toujours préparer plusieurs échantillons pour l'attaque, et de réaliser des tests en observant la surface au microscope optique immédiatement après attaque

. Après-l-'attaque-beraha-réalisée-sur-la-tranche, six images sont acquises en microscopie optique : deux proches de la surface, deux à coeur de la tôle, et deux à quart d'épaisseur. Ensuite, une analyse par différence de niveaux de gris à l'aide du logiciel Stream Essentials d'Olympus est réalisée

, Cette méthode fait partie d'un savoir-faire en termes de caractérisations du centre de recherche d'Aperam. Pour davantage de détails