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eq.) was dissolved in pyridine (1 mL for 1 g of PEG) at 0°C. A solution of tosyl chloride (3.6 eq.) in pyridine (0.3 mL for 1 mmol of tosyl chloride) was then added slowly at -5ºC. The mixture was stirred for 4 to 48 h at 0ºC, and treated by adding ice with a 6N HCl solution ,
mg) was dissolved in a CH 2 Cl 2 /TFA 3:1 mixture (50 mL) and stirred at room temperature After 2 hours, the mixture was evaporated, dichloromethane (100 mL) was added and the solution was washed with a, 2000. ,
1 Hz, 2H); 13 C NMR (CDCl 3 , 400 MHz, 25°C): ? = 157, p.71 ,
91 mmol) was dissolved in CHCl 3 (10 mL) with PEG 11 OH (2000 mg, 1 eq., 3,64 mmol) and stirred at room temperature After 2 hours, brine (5 mL) was added and the mixture was stirred for 15 minutes. Layers were separated and the organic phase was dried with sodium sulfate and evaporated, 1769. ,
18 mmol) in CHCl 3 (200 mL) was added to 4-formylbenzoic acid (3276 mg, 1,2 eq., 21,82 mmol), EDC,HCl (3834 mg, 1,1 eq mmol) and the mixture was stirred for 12 h. The solution was then washed with HCl 0, DMAP (2443 mg, 1,1 eq with NaHCO, p.1, 2024. ,
07 (s, 3H); 13 C NMR (CDCl 3 , 400 MHz, 25°C): ? = 190 ,
16 mmol) and hydroxylamine hydrochloride (828 mg, 1,3 eq91 mmol) were dissolved in water/isopropylalcool mixture 1:1 (50 mL) at room temeprature. Sodium hydroxide (440 mg, 1.2 eq., 10,99 mmol) was then added and the mixture was stirred for 3 days. The mixture was then evaporated under vacuum, 2000. ,
00 (s, 1H), 3.86 (t, J = 6.5 Hz, 2H), 3, pp.73-76 ,
48 (s, 1H), 5.15 (s, 1H), pp.75-79 ,
ESI-MS: calcd for C 44 H 80, p.81 ,
(m, 16H); ESI-MS: Calcd for C 61 H 115, pp.9778-9781 ,
96 (t, J = 6.6 Hz, pp.77-80 ,
95 (t, J = 6.6 Hz, pp.82-85 ,
WT%) was dissolved in deuterium oxide (95 WT%) at room temperature. The dynamic profragrance (1 WT%) was added to the formulation at the beginning of the experiment (t=0), pH was measured and NMR measurements were launched ,