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le temps d'induction est régi par la croissance des nuclei jusqu'à une taille détectable. t ind est alors déduit de l'intégration des expressions cinétiques de la vitesse linéaire de croissance entre le rayon critique des germes et le rayon visible des germes ,
Elle sera égale à -1 pour une croissance normale et à -2 pour une croissance en spirale. Si la pente est inférieure à - 2, on suppose que le mécanisme de croissance est de type B+S. Pour la croissance bidimensionnelle, la courbe ln ,
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un cristal sont des plans réticulaires particulièrement denses en noeuds, donc appartenant à des familles où la distance inter réticulaire est grande. Par conséquent les arrêtes sont des rangées denses du réseau (loi d'observation) Il est utile de faire remarquer que les faces qui se développent dans un cristal, sont celles dont la croissance est lente (vitesse de croissance dans la direction de la normale à la face) Si une face croît lentement c'est que les plans réticulaires qui la Structural and kinetic features of crystal growth inhibition: adipic acid growing in the presence of n-alkanoic acids, Journal of the Chemical Society Faraday Transactions, vol.88, issue.23, p.3461, 1992. ,
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situ peut fournir des informations quantitatives sur la distribution en taille des particules. Par ailleurs, d'un point de vue qualitatif, elle permet de mettre en évidence les mécanismes de cristallisation. La Figure 3-9 montre l'évolution des images obtenues au cours d'une cristallisation par refroidissement non ensemencée de l'oxalate d'ammonium monohydrate. On peut y observer par exemple les cristaux issus de la nucléation primaire homogène, puis l'apparition de fines particules caractéristiques d'un mécanisme de nucléation secondaire (non représentées ici) (a) (b) ,
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