40 mm) et partiellement saturé Résultats de perméabilité apparente. La Fig. 4.30 permet de visualiser la variation de perméabilité apparente K app en fonction de la température lors du seul cycle de chauffage jusqu'à 200 o C de cet échantillon. A partir de 150 o C (température du béton) et jusqu'à 180 o C, le capteur de pression situé en amont de l'échantillon montre que le gaz ne peut plus passer par le réseau poreux. Comme pour l'échantillon Gris N o -4L, la pression d'injection de gaz ne diminue plus, elle augmente même petit à petit ,
échantillon est replacé en étuve à 105 o C, pour vérifier s'il contient encore de l'eau libre Après 12 jours en étuve à 105 o C, l'échantillon a perdu seulement 0,1g : on peut dire qu'il n'y avait plus réellement d'eau libre dans l'échantillon après chauffage jusqu ,
effet Klinkenberg, car la valeur de ? calculée est négative, voir la Fig. 4.31. L'interprétation est la même que pour les essais précédents. On trouve une perméabilité apparente très faible, de l'ordre de 10 ?19 m 2 . Par contre, à 200 o C, la perméabilité intrinsèque K int vaut 3,98×10 ?18 m 2 : cet échantillon, après avoir été chauffé à 200 o C, est beaucoup plus perméable qu'à l'état initial. Le coefficient de Klinkenberg ? est égal à 0,653MPa. Mais en l'absence d'effet Klinkenberg à température ambiante ,
et que la perméabilité augmente légèrement avec la pression d'injection . Par contre, en fin de cycle, lorsque l'on revient à la température ambiante, la perméabilité intrinsèque est beaucoup plus élevée par rapport à la valeur initiale : K int vaut 2, pp.55-65 ,
effet de structure sur l'existence de l'effet bouchon : il existe même sur un échantillon beaucoup plus court (40mm de long et toujours 65mm de diamètre) Il dure également longtemps (plusieurs heures) ,
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