diyl)bisphosphonatede tétraéthyle 70 -Synthèse du 5,5-bisdiéthoxy phosphoryl-3,4-dihydro-2H-pyrrole-1-oxyde (DPBO), Via la synthèse en une étape de ,
162 3.2.1.3. Piégeage du radical méthyle et du radical CO 2, DIHYDRO-2H-PYRROLE-1-OXYDE (DEPMPO-PH) 6 ,
Conclusion sur les différentes études portant sur les nitroxydes 70NO, pp.73-90 ,
[35] Comparative studies on different methods of malonaldehyde determination, Methods in Enzymology, vol.105, pp.299-305, 1984. ,
DOI : 10.1016/S0076-6879(84)05038-2
Molecular oxygen: Friend and foe*The role of the oxygen free radical system in the calcium paradox, the oxygen paradox and ischemia/reperfusion injury, Journal of Molecular and Cellular Cardiology, vol.16, issue.11, pp.969-985, 1984. ,
DOI : 10.1016/S0022-2828(84)80011-5
Radicals in Aqueous Solution, Journal of Physical and Chemical Reference Data, vol.14, issue.4, pp.1041-1100, 1985. ,
DOI : 10.1063/1.555739
A Molecular Biologic Approach to Cardiac Toxicology, Adv. Exp. med. Biol, vol.161, pp.509-518, 1983. ,
DOI : 10.1007/978-1-4684-4472-8_30
Free radicals, cardiovascular dysfunction and protection strategies, Landes Company: Austin, 1994. ,
DOI : 10.1016/0891-5849(94)90084-1
Oxygen-mediated myocardial damage during ischameia and reperfusion: Role of the cellular defences against oxygen toxicity, Journal of Molecular and Cellular Cardiology, vol.17, issue.10, pp.937-945, 1985. ,
DOI : 10.1016/S0022-2828(85)80074-2
beta-Carotene: an unusual type of lipid antioxidant, Science, vol.224, issue.4649, pp.569-573, 1984. ,
DOI : 10.1126/science.6710156
Catalyseurs du monde vivant; Presses universitaires de Grenoble: Grenoble, 1995. ,
In Oxidative Stress; H. Sies, pp.151-195, 1985. ,
Antioxidants in Human Health and Disease, Annual Review of Nutrition, vol.16, issue.1, pp.33-50, 1996. ,
DOI : 10.1146/annurev.nu.16.070196.000341
The integrated antioxidant system, Nutrition Research, vol.15, issue.5, pp.755-766, 1995. ,
DOI : 10.1016/0271-5317(95)00041-G
Oxidative Stress; H. Sies, pp.197-218, 1985. ,
[41] Fluorescent damage products of lipid peroxidation, Methods in Enzymology, vol.105, pp.337-341, 1984. ,
DOI : 10.1016/S0076-6879(84)05044-8
A method for the detection of superoxide in biological systems, Archives of Biochemistry and Biophysics, vol.215, issue.2, pp.367-378, 1982. ,
DOI : 10.1016/0003-9861(82)90097-2
[51] Measurement of oxidizing radicals by polymorphonuclear leukocytes, Methods in Enzymology, vol.105, pp.393-398, 1984. ,
DOI : 10.1016/S0076-6879(84)05054-0
[68] Microsomal oxidant radical production and ethanol oxidation, Methods in Enzymology, vol.105, pp.516-522, 1984. ,
DOI : 10.1016/S0076-6879(84)05071-0
Detection of radical adducts of 5,5-dimethyl-1-pyrroline N-oxide by the combined use of high-performance liquid chromatography with electrochemical detection and electron spin resonance, Analytical Biochemistry, vol.196, issue.1, pp.111-119, 1991. ,
DOI : 10.1016/0003-2697(91)90126-E
[33] Overview of methods used for detecting lipid peroxidation, Methods in Enzymology, vol.105, issue.56, pp.283-293, 1984. ,
DOI : 10.1016/S0076-6879(84)05036-9
[34] Chemical methods for the detection of lipid hydroperoxides, Methods in Enzymology, vol.105, pp.293-299, 1984. ,
DOI : 10.1016/S0076-6879(84)05037-0
Persistent carbon-centered radicals, Accounts of Chemical Research, vol.9, issue.1, pp.13-19, 1976. ,
DOI : 10.1021/ar50097a003
Advances in Physical Organic Chemistry, pp.1-64, 1980. ,
Kinetic applications of electron paramagnetic resonance spectroscopy. III. Self-reactions of dialkyl nitroxide radicals, Journal of the American Chemical Society, vol.93, issue.24, pp.6555-6561, 1971. ,
DOI : 10.1021/ja00753a038
The captodative effect, Accounts of Chemical Research, vol.18, issue.5, pp.148-154, 1985. ,
DOI : 10.1021/ar00113a004
Advances In Free Radicals Chemistry, pp.189-317, 1975. ,
Electron paramagnetic resonance of free radicals in an adamantane matrix. III. Isocyanatoalkyl and isothiocyanatoalkyl radicals, Journal of the American Chemical Society, vol.93, issue.17, pp.4145-4148, 1971. ,
DOI : 10.1021/ja00746a008
Electron Spin Resonance Studies of Free Radicals and Their Reactions in Aqueous Solution; Special publication of the Chemical Society, pp.117-145, 1970. ,
Studies on the Origin of the Hydroxyl Spin Adduct of DMPO Produced from the Stimulation of Neutrophils by Phorbol-12-Myristate-13-Acetate, Free Radical Research Communications, vol.81, issue.2, pp.115-154, 1980. ,
DOI : 10.1016/0014-5793(78)80116-1
Spin trapping of superoxide and hydroxyl radical: Practical aspects, Archives of Biochemistry and Biophysics, vol.200, issue.1, pp.1-16, 1980. ,
DOI : 10.1016/0003-9861(80)90323-9
Considerations in the spin trapping of superoxide and hydroxyl radical in aqueous systems using 5,5-dimethyl-1-pyrroline-1-oxide, Biochemical and Biophysical Research Communications, vol.83, issue.1, pp.69-74, 1978. ,
DOI : 10.1016/0006-291X(78)90398-4
Problems associated with spin trapping oxygen-centered free radicals in biological systems, Analytical Biochemistry, vol.177, issue.1, pp.1-6, 1989. ,
DOI : 10.1016/0003-2697(89)90002-X
[9] Spin-trapping methods for detecting superoxide and hydroxyl free radicals in vitro and in vivo, Methods in Enzymology, vol.186, pp.127-133, 1990. ,
DOI : 10.1016/0076-6879(90)86101-Z
Detection of peroxyl and alkoyl radicals produced by reaction of hydroperoxides with heme-proteins by electron spin resonance spectroscopy, Biochimica et Biophysica Acta (BBA) - General Subjects, vol.964, issue.1, pp.28-35, 1988. ,
DOI : 10.1016/0304-4165(88)90063-3
Superoxide-dependent lipid peroxidation. Problems with the use of catalase as a specific probe for fenton-derived hydroxyl radicals, Biochemical and Biophysical Research Communications, vol.117, issue.3, pp.901-907, 1983. ,
DOI : 10.1016/0006-291X(83)91681-9
Comprehensive Organic Synthesis, pp.551-569, 1991. ,
Comprehensive Organic Synthesis, 1991. ,
Intramolecular Cyclizations from N-alkoxyamines. Formation of Dialkylsubstituted pyrrolidines and piperidines, Tetrahedron Letters, vol.30, issue.11, pp.1327-1330, 1989. ,
DOI : 10.1016/S0040-4039(00)99456-5
Synthesis of carbon-phosphorus bonds, N. Chem. Abs. J. Org. Chem, vol.97, issue.38, pp.72582-72619, 1973. ,
Résultats non publiés (39) Coutrot, P.; Snoussi, M.; Savignac, P. Synthesis, pp.133-134, 1978. ,
The Reformatsky Reaction with Benzalaniline, Journal of the American Chemical Society, vol.65, issue.11, pp.2255-2256, 1943. ,
DOI : 10.1021/ja01251a503
The Reaction of Chloral with Cyclohexylmagnesium Bromide, Journal of the American Chemical Society, vol.65, issue.11, pp.2255-2301, 1943. ,
DOI : 10.1021/ja01251a502
Rate constants for aryl radical cyclization to aldimines: synthesis of tetrahydroisoquinolines by fast 6-endo closures to carbon, Tetrahedron Letters, vol.33, issue.16, pp.2123-2126, 1992. ,
DOI : 10.1016/0040-4039(92)88156-Y
Animation reductrice des ??-cetophosphonates: preparation d'acides aminoalkylphosphoniques, Tetrahedron, vol.37, issue.21, pp.3713-3721, 1981. ,
DOI : 10.1016/S0040-4020(01)98903-3
Peracid oxidation of aliphatic amines: general synthesis of nitroalkanes, The Journal of Organic Chemistry, vol.44, issue.4, pp.659-661, 1979. ,
DOI : 10.1021/jo01318a050
Addition Reactions of Nitroalkanes with Acrolein and Methyl Vinyl Ketone. Selective Reduction of Nitrocarbonyl Compounds to Nitrocarbinols, Journal of the American Chemical Society, vol.74, issue.14, pp.3664-3668, 1952. ,
DOI : 10.1021/ja01134a058
A new synthesis of macrocyclic keto-lactones via ring expansion of 2-(3-hydroxypropyl)-2-nitrocycloalkanones, Tetrahedron Letters, vol.23, issue.34, pp.3521-3524, 1982. ,
DOI : 10.1016/S0040-4039(00)87658-3
Reactions of resonance stabilized anions. 34. Synthesis of nitrocyclopropanes by cyclization of .gamma.-chloro-.gamma.-nitro carboxylic esters and derivatives, The Journal of Organic Chemistry, vol.44, issue.8, pp.1195-1199, 1979. ,
DOI : 10.1021/jo01322a001
New synthetic methods. Conjugate addition of alkyl groups to electron deficient olefins with nitroalkanes as alkyl anion equivalents, The Journal of Organic Chemistry, vol.50, issue.20, pp.3692-3698, 1985. ,
DOI : 10.1021/jo00220a003
Synthesis of homochiral 4-amino-4-carboxy-2-phosphonomethylpyrrolidines via a diastereoselective bucherer-bergs reaction of 4-oxopyrrolidine derivative: Novel conformationally restricted AP 5 analogues, Tetrahedron: Asymmetry, vol.6, issue.9, pp.2271-2279, 1995. ,
DOI : 10.1016/0957-4166(95)00302-6
Preparation of activated imines and their condensation with allylstannanes: stereoselective synthesis of 1,2-amino alcohols, The Journal of Organic Chemistry, vol.54, issue.20, pp.4739-4741, 1989. ,
DOI : 10.1021/jo00281a008
TMSO-triflate-assisted addition of enols to heteroaromatic imines or hydroxyaminal intermediates, Tetrahedron Letters, vol.35, issue.37, pp.6883-6886, 1994. ,
DOI : 10.1016/0040-4039(94)85031-3
Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes, The Journal of Organic Chemistry, vol.39, issue.8, pp.1017-1028, 1974. ,
DOI : 10.1021/jo00922a001
KINETICS AND MECHANISM OF THE BECKMANN REARRANGEMENT OF ALICYCLIC KETOXIMES UNDER THE CATALYTIC ACTION OF SULPHURIC ACID AND OLEUM, Russian Chemical Reviews, vol.36, issue.1, pp.51-64, 1967. ,
DOI : 10.1070/RC1967v036n01ABEH001583
Photochemistry of Oximes III. The Photochemical Beckmann Rearrangement, Canadian Journal of Chemistry, vol.49, issue.17, pp.2891-2896, 1971. ,
DOI : 10.1139/v71-479
Considerations in the spin trapping of superoxide and hydroxyl radical in aqueous systems using 5,5-dimethyl-1-pyrroline-1-oxide, Biochemical and Biophysical Research Communications, vol.83, issue.1, pp.69-74, 1978. ,
DOI : 10.1016/0006-291X(78)90398-4
Advances in Physical Organic Chemistry, pp.1-64, 1980. ,
Pentamethoxynitrosobenzene: (MeO)5phNO. A useful new spin-trapping agent, Tetrahedron Letters, vol.25, issue.21, pp.2215-2218, 1984. ,
DOI : 10.1016/S0040-4039(01)80214-8
Synthesis, redox behavior and spin-trap properties of 2,6-di-tert-butylnitrosobenzene (DTBN), The Journal of Organic Chemistry, vol.54, issue.6, pp.1447-1450, 1989. ,
DOI : 10.1021/jo00267a041
Electron spin resonance studies of radical trapping in the radiolysis of organic liquids. I. Evidence for the primary formation of the methoxy radical in methanol, Journal of the American Chemical Society, vol.94, issue.22, pp.7917-7918, 1972. ,
DOI : 10.1021/ja00777a040
Oxygen free radicals in ischemic acute renal failure in the rat., Journal of Clinical Investigation, vol.74, issue.4, pp.1156-1164, 1984. ,
DOI : 10.1172/JCI111524
Detection and identification of short-lived free radicals by an electron spin resonance trapping technique, Journal of the American Chemical Society, vol.90, issue.21, pp.5909-5910, 1968. ,
DOI : 10.1021/ja01023a051
Detection and identification of short-lived free radicals by electron spin resonance trapping techniques (spin trapping). Photolysis of organolead, -tin, and -mercury compounds, Journal of the American Chemical Society, vol.91, issue.16, pp.4481-4490, 1969. ,
DOI : 10.1021/ja01044a028
Nitrile Oxides, Nitrones, and Nitronates in Organic Synthesis. Novel Strategies in Synthesis, 1988. ,
Spin trapping of superoxide and hydroxyl radicals with substituted pyrroline 1-oxides, Journal of Medicinal Chemistry, vol.29, issue.12, pp.2439-2444, 1986. ,
DOI : 10.1021/jm00162a004
Biological spin trapping methodology. III. Octanol-water partition coefficients of spin-trapping compounds, Journal of Biochemical and Biophysical Methods, vol.32, issue.3, pp.183-190, 1996. ,
DOI : 10.1016/0165-022X(96)00008-5
Identification of Reactive Free Radicals with a New 31P-Labeled DMPO Spin Trap, The Journal of Organic Chemistry, vol.60, issue.17, pp.5441-5445, 1995. ,
DOI : 10.1021/jo00122a022
Spin Trapping: ESR parameters of spin adducts 1474 1528V, Free Radical Biology and Medicine, vol.3, issue.4, pp.259-303, 1987. ,
DOI : 10.1016/S0891-5849(87)80033-3
EPR Spin-Trapping Study of the Sonolysis of H2O/D2O Mixtures: Probing the Temperatures of Cavitation Regions, The Journal of Physical Chemistry, vol.99, issue.11, pp.3605-3611, 1995. ,
DOI : 10.1021/j100011a030
Formation of the DMPO-OH adduct from Ti(IV) and DMPO in aqueous solution ??? the first ESR evidence, Inorganica Chimica Acta, vol.234, issue.1-2, pp.169-171, 1995. ,
DOI : 10.1016/0020-1693(95)04468-O
Synthesis and Spin-Trapping Chemistry of 5,5-Dimethyl-2-(trifluoromethyl)-1-pyrroline N-Oxide, The Journal of Organic Chemistry, vol.60, issue.17, pp.5434-5440, 1995. ,
DOI : 10.1021/jo00122a021
New 2-substituted pyrroline-N-oxides: An EPR solvent study of the radical spin adducts, Magnetic Resonance in Chemistry, vol.54, issue.12, pp.711-720, 1994. ,
DOI : 10.1002/mrc.1260321203
Studies on the stability of oxygen radical spin adducts of a new spin trap: 5-methyl-5-phenylpyrroline-1-oxide (MPPO), Free Radical Biology and Medicine, vol.21, issue.6, pp.889-894, 1996. ,
DOI : 10.1016/0891-5849(96)00232-8
EPR spin-trapping study on the oxidizing species formed in the reaction of the ferrous ion with hydrogen peroxide, Journal of the American Chemical Society, vol.113, issue.20, pp.7588-7593, 1991. ,
DOI : 10.1021/ja00020a021
[23] Spin trapping of superoxide and hydroxyl radicals, J. Methods in Enzymology, vol.105, pp.198-209, 1984. ,
DOI : 10.1016/S0076-6879(84)05026-6
Radicals in Aqueous Solution, Journal of Physical and Chemical Reference Data, vol.14, issue.4, pp.1041-1100, 1985. ,
DOI : 10.1063/1.555739
A method for the detection of superoxide in biological systems, Archives of Biochemistry and Biophysics, vol.215, issue.2, pp.367-378, 1982. ,
DOI : 10.1016/0003-9861(82)90097-2
Detection of radical adducts of 5,5-dimethyl-1-pyrroline N-oxide by the combined use of high-performance liquid chromatography with electrochemical detection and electron spin resonance, Analytical Biochemistry, vol.196, issue.1, pp.111-119, 1991. ,
DOI : 10.1016/0003-2697(91)90126-E
Spin trapping of superoxide and hydroxyl radical: Practical aspects, Archives of Biochemistry and Biophysics, vol.200, issue.1, pp.1-16, 1980. ,
DOI : 10.1016/0003-9861(80)90323-9
Problems associated with spin trapping oxygen-centered free radicals in biological systems, Analytical Biochemistry, vol.177, issue.1, pp.1-6, 1989. ,
DOI : 10.1016/0003-2697(89)90002-X
[9] Spin-trapping methods for detecting superoxide and hydroxyl free radicals in vitro and in vivo, Methods in Enzymology, vol.186, pp.127-133, 1990. ,
DOI : 10.1016/0076-6879(90)86101-Z
Detection of peroxyl and alkoyl radicals produced by reaction of hydroperoxides with heme-proteins by electron spin resonance spectroscopy, Biochimica et Biophysica Acta (BBA) - General Subjects, vol.964, issue.1, pp.28-35, 1988. ,
DOI : 10.1016/0304-4165(88)90063-3
Spin trapping. Kinetics of the reaction of superoxide and hydroxyl radicals with nitrones, Journal of the American Chemical Society, vol.102, issue.15, pp.4994-4999, 1980. ,
DOI : 10.1021/ja00535a029
-oxide in Fenton systems. Characterization of key precursors giving rise to background ESR signals, Canadian Journal of Chemistry, vol.70, issue.11, pp.2818-2827, 1992. ,
DOI : 10.1139/v92-358
URL : https://hal.archives-ouvertes.fr/in2p3-00932021
Solvent effects on the nitrogen and β-hydrogen hyperfine splitting constants of aminoxyl radicals obtained in spin trapping experiments, Canadian Journal of Chemistry, vol.60, issue.21, pp.2725-2733, 1982. ,
DOI : 10.1139/v82-392
Evidence against the 1:2:2:1 quartet DMPO spectrum as the radical adduct of the lipid alkoxyl radical, Archives of Biochemistry and Biophysics, vol.296, issue.2, pp.645-649, 1992. ,
DOI : 10.1016/0003-9861(92)90621-3
Spin trapping of radicals formed during radiolysis of aqueous solutions. Direct electron spin resonance observations, Canadian Journal of Chemistry, vol.54, issue.2, pp.275-279, 1976. ,
DOI : 10.1139/v76-041
Synthèse d'une nouvelle nitrone phosphorylée: la 5-diéthoxyphosphoryl-5- méthyl-1-pyrroline N-oxide (DEPMPO) Applications au piégeage in vitro et in vivo des radicaux libres centrés sur l'oxygène, Thèse de Chimie Organique, 1994. ,
Electron Spin Resonance Studies of Free Radicals and Their Reactions in Aqueous Solution; Special publication of the Chemical Society, pp.117-145, 1970. ,
Oxygen radicals and the nervous system, Trends in Neurosciences, vol.8, pp.22-26, 1985. ,
DOI : 10.1016/0166-2236(85)90010-4
The chemistry of superoxide ion, Tetrahedron, vol.35, issue.12, pp.1471-1481, 1979. ,
DOI : 10.1016/0040-4020(79)80032-0
Radical Chemistry, Bull. Soc. Chim. Fr, vol.128, pp.505-520, 1991. ,
ESR Spin Trapping Study of Sodium and Tetramethylammonium Mercaptoundecahydro-closo-dodecaborates(2-) and Sodium Tetraborate Aqueous Solutions Irradiated by UV Light at Room Temperature, Collection of Czechoslovak Chemical Communications, vol.60, issue.5, pp.851-855, 1995. ,
DOI : 10.1135/cccc19950851
Free Radical Production by Sonolysis of Aqueous Mixtures of N,N-Dimethylformamide: An EPR Spin Trapping Study, The Journal of Physical Chemistry, vol.99, issue.16, pp.5970-5976, 1995. ,
DOI : 10.1021/j100016a037
Formation of Aminoxyl Radicals in Alkaline Water Solutions from Spin Traps and Short-Lived Radicals Derived from Some CH-Acidic Compounds., Acta Chemica Scandinavica, vol.49, issue.65, pp.399-404, 1995. ,
DOI : 10.3891/acta.chem.scand.49-0399
Electron spin resonance and pulse radiolysis studies on the spin trapping of sulphur-centered radicals, Chemico-Biological Interactions, vol.61, issue.2, pp.177-188, 1987. ,
DOI : 10.1016/0009-2797(87)90038-X
Simulation of Multiple Isotropic Spin-Trap EPR Spectra, Journal of Magnetic Resonance, Series B, vol.104, issue.2, pp.105-110, 1994. ,
DOI : 10.1006/jmrb.1994.1062
Automatic computer simulations of ESR spectra, Applied Magnetic Resonance, vol.38, issue.1-3, pp.29-43, 1996. ,
DOI : 10.1007/BF03163097
Résultats non publiés (78) Castellano, S.; Bothner-By, A. Computer Programs for Chemistry, pp.10-39 ,
Kinetic applications of electron paramagnetic resonance spectroscopy. III. Self-reactions of dialkyl nitroxide radicals, Journal of the American Chemical Society, vol.93, issue.24, pp.6555-6561, 1971. ,
DOI : 10.1021/ja00753a038
Kinetic applications of electron paramagnetic resonance spectroscopy. II. Self-reactions of N-alkyl nitroxides and N-phenyl nitroxide, Journal of the American Chemical Society, vol.93, issue.24, pp.6551-6555, 1971. ,
DOI : 10.1021/ja00753a037
Chiral Spin Traps. The Spin Trapping Chemistry of 5-Methyl-5-phenylpyrroline-N-oxide (MPPO), Journal of Magnetic Resonance, Series B, vol.111, issue.3, pp.254-263, 1991. ,
DOI : 10.1006/jmrb.1996.0091
Synthesis of a Novel Nitrone, 2-Phenyl-5,5-dimethyl-1-pyrroline N-Oxide (nitronyl-13C), for Enhanced Radical Addend Recognition and Spin Adduct Persistence, Journal of the American Chemical Society, vol.116, issue.9, pp.3738-3743, 1994. ,
DOI : 10.1021/ja00088a009
Stability constants of some complexes of t-butyl mesityl nitroxide, Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, vol.69, issue.0, pp.864-870, 1973. ,
DOI : 10.1039/f19736900864
In Handbook of experimental pharmacology, pp.440-466, 1988. ,
MHz12 MHz MHz), p.40061 ,
Silicagel 60, 230-400 mesh". Les révélateurs utilisés sont l'éclairage UV et l'acide phosphomolybdique en solution dans l'éthanol, 8H, -O-C H 2 - CH 3 ) ppm, p.69428817 ,
HN-C H 2 -CH 2 -CH 2 -C) On laisse sous agitation à température ambiante pendant 21 heures. L'éthanol est évaporé sous pression réduite et le brut repris par 150 ml de dichlorométhane. La phase organique est lavée successivement par une solution aqueuse (20 ml) d'acide chlorhydrique 12 N, une solution aqueuse saturée en NaHCO 3 (20 ml), de l'eau (2 fois 20 ml) et par une solution aqueuse saturée en NaCl (2 fois 20 ml). On sèche sur Na 2 SO 4 et après filtration et reconcentration on obtient 27, p.0 ,
Les concentrations sont : [Nitrone] = 10 mM ,
Palladium-catalyzed cyclization of .omega.-olefinic tosamides. Synthesis of nonaromatic nitrogen heterocycles, Journal of the American Chemical Society, vol.104, issue.9, pp.2444-2449, 1982. ,
DOI : 10.1021/ja00373a019
Animation reductrice des ??-cetophosphonates: preparation d'acides aminoalkylphosphoniques, Tetrahedron, vol.37, issue.21, pp.3713-3721, 1981. ,
DOI : 10.1016/S0040-4020(01)98903-3
A more efficient synthesis of DMPO-type (Nitrone) spin traps, The Journal of Organic Chemistry, vol.51, issue.22, pp.4298-4300, 1986. ,
DOI : 10.1021/jo00372a039
Nuclear magnetic resonance spectroscopy. Use of carbon-13 spectra to establish configurations of oximes, The Journal of Organic Chemistry, vol.39, issue.8, pp.1017-1028, 1974. ,
DOI : 10.1021/jo00922a001
Synthesis of fused 1,2-diazetidinones via an intramolecular Horner-Emmons reaction, The Journal of Organic Chemistry, vol.51, issue.9, pp.1537-1540, 1986. ,
DOI : 10.1021/jo00359a029
New synthetic methods. Conjugate addition of alkyl groups to electron deficient olefins with nitroalkanes as alkyl anion equivalents, The Journal of Organic Chemistry, vol.50, issue.20, pp.3692-3698, 1985. ,
DOI : 10.1021/jo00220a003
Trialkyl ??-Phosphonates, Journal of the American Chemical Society, vol.79, issue.24, pp.6524-6526, 1957. ,
DOI : 10.1021/ja01581a044
New 2-substituted pyrroline-N-oxides: An EPR solvent study of the radical spin adducts, Magnetic Resonance in Chemistry, vol.54, issue.12, pp.711-720, 1994. ,
DOI : 10.1002/mrc.1260321203
Synthesis of a Novel Nitrone, 2-Phenyl-5,5-dimethyl-1-pyrroline N-Oxide (nitronyl-13C), for Enhanced Radical Addend Recognition and Spin Adduct Persistence, Journal of the American Chemical Society, vol.116, issue.9, pp.3738-3743, 1994. ,
DOI : 10.1021/ja00088a009
In Vogel's Textbook of pratical organic chemistry, pp.815-816, 1978. ,
Asymmetric Michael reaction of ??-cyano carboxylates catalyzed by a rhodium complex with trans-chelating chiral diphosphine PhTRAP, Tetrahedron, vol.50, issue.15, pp.4439-4454, 1994. ,
DOI : 10.1016/S0040-4020(01)89377-7
Synthesis and properties of some nitroxide .alpha.-carboxylate salts, The Journal of Organic Chemistry, vol.54, issue.10, pp.2417-2420, 1989. ,
DOI : 10.1021/jo00271a033
Synthèse d'une nouvelle nitrone phosphorylée: la 5-diéthoxyphosphoryl-5- méthyl-1-pyrroline N-oxide (DEPMPO) Applications au piégeage in vitro et in vivo des radicaux libres centrés sur l'oxygène, Thèse de Chimie Organique, 1994. ,
Nitroxyde ?-phosphorylés -Application a la polymérisation, Thèse de Chimie Organique, 1997. ,
Sources de production in vivo du radical anion superoxyde : rôle de la xanthine oxydase (XO), p.20 ,
26 ?. ?-Carotène 40, p.27 ,
53 ? Protection sous forme de carbamate54 * Sous forme de carbamate de méthyle, p.56 ,
59 f. Création d'une liaison carbone-phosphore à partir d'un halogénure, Cyclisation induite par les ions mercurinium, p.59 ,
Via la réduction d'un groupement nitro (Voie n°3), p.64 ,
70 ? Préparation d'un groupement libérable (Schéma 2-47), p.70 ,
-iodométhyl-2-méthyltétraméthylène)carbamate de benzyle 21, p.71 ,
111 ? Passage par une dicétolactone, p.111 ,
120 ? Méthode A (condition douce), p.121 ,
145 * la PBN et ses homologues, p.145 ,
Antal Rockenbauer 75, p.157 ,
Discipline Chimie Organique Mots-Clés : Nitrone, Phosphore, Spin-Trapping, p.521 ,